Details
2,2,2-TRIFLUOROETHANOL-D3 77253-67-9 with purity >99% Low price in stock
- Molecular Formula: C2D3F3O
- Molecular Weight: 103.017
- Appearance/Colour: clear colorless liquid
- Vapor Pressure: 77.3mmHg at 25°C
- Melting Point: -44 °C(lit.)
- Refractive Index: n20/D 1.3(lit.)
- Boiling Point: 74 °C at 760 mmHg
- Flash Point: 29.4 °C
- PSA： 20.23000
- Density: 1.415 g/mL at 25 °C(lit.)
- LogP: 0.54100
2,2,2-TRIFLUOROETHANOL-D3(Cas 77253-67-9) Usage
|
General Description |
2,2,2-Trifluoroethanol-d3 (TFEd3) is 2,2,2-trifluoroethanol in which hydrogen of the –OH group is substituted with deuterium. It is a commonly used 1H NMR and 13C NMR solvent. |
InChI:InChI=1/C2H3F3O/c3-2(4,5)1-6/h6H,1H2/i1D2,6D
77253-67-9 Relevant articles
Simple and efficient catalytic reaction for the selective deuteration of alcohols
Khaskin, Eugene,Milstein, David
, p. 448 - 452 (2013/08/25)
A highly efficient system for the cataly...
METHOD FOR PRODUCING DEUTERATED PERFLUOROALYKYL METHANOL
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Page/Page column 7-8, (2008/06/13)
PROBLEM TO BE SOLVED: To provide a metho...
77253-67-9 Process route
-
-
75-89-8
2,2,2-trifluoroethanol
-
-
77253-67-9
trifluoroethanol-d3
| Conditions | Yield |
|---|---|
|
With
(6-di-tert-butylphosphinomethyl-2,2’-bipyridyl)Ru(CO)HCl; water-d2; sodium hydroxide;
at 135 ℃;
for 40h;
|
18 %Spectr.
|
-
-
407-25-0
trifluoroacetic anhydride
-
-
77253-67-9
trifluoroethanol-d3
| Conditions | Yield |
|---|---|
|
With
deuterium hydride;
Ru/C;
at 160 ℃;
for 5.5h;
Product distribution / selectivity;
|
79%
|
77253-67-9 Upstream products
-
407-25-0
trifluoroacetic anhydride
-
75-89-8
2,2,2-trifluoroethanol
77253-67-9 Downstream products
-
7448-86-4
1-(4-methoxyphenyl)prop-2-en-1-one
-
18293-99-7
Prenyltrimethylsilane
-
18294-00-3
trimethyl-(3-methyl-but-3-enyl)-silane
-
74-85-1
ethene
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